huagongshe.com
HRID410042

反应详情

EQUATION

反应方程式

HRID 410042 的结构方程式

REACTANTS

反应物

2
结构：Oc1cccc(O)c1
HCID5054

Resorcinol

C6H6O2

结构：COC(=O)c1ccc(CC(=O)O)c(C)c1
HCID57555224

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(CC(=O)c2ccc(O)cc2O)c(C)c1
HCID67367578

未命名化合物

收率 69.6%

PROCEDURE

实验过程

2-(4-(methoxycarbonyl)-2-methylphenyl)acetic acid (295 mg) was treated with resorcinol (190 mg) in BF3Et2O at 90° C. over night. After aqueous work-up with ethyl acetate and column purification, the desired product (296 mg) was isolated as an oil.

WORKUP

后处理

  1. customAfter aqueous work-up with ethyl acetate and column purification