Hydrochloric Acid → HCID 131723885, compound

HRID 412151Notes

Reaction equation

HRID 412151 reaction equation
C(OC([N:8]1[CH2:13][CH2:12][N:11]([C:14](=[O:27])[CH2:15][C:16]2[CH:21]=[CH:20][CH:19]=[C:18]([O:22][S:23]([CH3:26])(=[O:25])=[O:24])[CH:17]=2)[CH2:10][CH2:9]1)=O)(C)(C)C.[ClH:28]>C(OCC)(=O)C>[ClH:28].[CH3:26][S:23]([O:22][C:18]1[CH:17]=[C:16]([CH2:15][C:14]([N:11]2[CH2:10][CH2:9][NH:8][CH2:13][CH2:12]2)=[O:27])[CH:21]=[CH:20][CH:19]=1)(=[O:24])=[O:25]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 18536039HCID 18536039, compound

Product 1

HCID 131723885HCID 131723885, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

Through a solution of the product from Step B (2.07 g, 5.22 mmol) in 75 mL of ethyl acetate at 0° C. was bubbled anhydrous HCl gas for 5 minutes. After 15 minutes, the reaction was concentrated in vacuo to produce the titled product as a white foam.

Workup

  1. concentrationthe reaction was concentrated in vacuo

Sources & evidence

ORD record
ord-8eaa18720eb5411692238fdf49e1a5f6
Source dataset
uspto-grants-2003_05
Patent number
US06562823B1

Reaction notes

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