反应详情

4-(Cyclohexylcarbamoylmethylamino)-3-nitrobenzonitrile (3.64 g) was hydrogenated using 7.5% palladium carbon (1.1 g) in tetrahydrofuran (100 ml) at atmospheric pressure over 40 min. After completion of the reaction, the reaction mixture was filtered through celite, and the solvent was evaporated and the residue was dried under reduced pressure to give the title compound (3.274 g).

1. customover 40 min
2. customAfter completion of the reaction
3. filtrationthe reaction mixture was filtered through celite
4. customthe solvent was evaporated
5. customthe residue was dried under reduced pressure