反应详情

Into a 4 liter autoclave were placed 425 g of sulfur, 75 g of DCPD, 2500 ml of water, 20 g of calcium carbonate and 5.0 g of Igepal®-630 (GAF). The reactor was sealed and heated to 150° for three hours with stirring. After cooling to room temperature, the sulfur/DCPD adduct was isolated as small ribbons.

1. customThe reactor was sealed
2. temperatureheated to 150° for three hours