反应详情

温度

140 °C

2,5-Dimethylindole (290 mg) and 8-methyl-4-chloroquinoline (360 mg) were suspended in N-methylpyrolidinone (0.5 ml), and maintained under a nitrogen atmosphere. The reaction was heated to 140° C. with stirring for 45 minutes. On cooling a deep red precipitate formed, the mixture was diluted with diethylether and the solid collected by filtration, and dried to give the sub-title compound (570 mg).

1. temperaturemaintained under a nitrogen atmosphere
2. temperatureOn cooling a deep red precipitate
3. customformed
4. filtrationthe solid collected by filtration
5. customdried