反应详情

A solution of 5-methyl-2-(6-morpholinopyridin-3-ylamino)benzoate tert-butyl ester in TFA (0.6 ml, 7.58 mmol) was stirred at room temperature for 1 hour. The solvent was evaporated and the residue was triturated in diethyl ether. The solid formed was filtered off to afford 0.047 g (73% of yield) of the expected product.

1. customThe solvent was evaporated
2. customthe residue was triturated in diethyl ether
3. customThe solid formed
4. filtrationwas filtered off
5. customto afford