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HRID423428

反应详情

EQUATION

反应方程式

HRID 423428 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：ClCCl
HCID6344

Dichloromethane

CH2Cl2

结构：N[C@@H]1CCN(c2ccc(-n3ccc4cc(-c5ccc(Cl)cc5)sc4c3=O)cn2)C1
HCID24758102

未命名化合物

PRODUCTS

生成物

1
结构：Cl.N[C@@H]1CCN(c2ccc(-n3ccc4cc(-c5ccc(Cl)cc5)sc4c3=O)cn2)C1
HCID24758101

未命名化合物

收率 93%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CCO
溶剂HCID702

Ethanol

C2H6O

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Prepare the HCl salt by dissolving the free base in MeOH and CH2Cl2 then adding 1N HCl in EtOH and evaporating. Suspend the salt in Et2O and filter to give 0.386 g (93%) of the title compound. MS/ES m/z (35Cl) 423.0 [M+H]+.

WORKUP

后处理

  1. customevaporating
  2. filtrationfilter