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HRID42628

反应详情

EQUATION

反应方程式

HRID 42628 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccncc1
HCID5922

Isonicotinic acid

C6H5NO2

结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

PRODUCTS

生成物

1
结构：Cl.O=C(Cl)c1ccncc1
HCID12262826

Pyridine-4-carbonyl chloride--hydrogen chloride (1/1)

C6H5Cl2NO

PROCEDURE

实验过程

A solution of isonicotinic acid (0.10 g, 0.8 mmol) and thionyl chloride (1 mL) were heated to reflux for 2 h and concentrated. The product obtained was used immediately in the following step.

WORKUP

后处理

  1. temperatureto reflux for 2 h
  2. concentrationconcentrated
  3. customThe product obtained