HRID426838

反应详情

EQUATION

反应方程式

HRID 426838 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 433 g. 2,5-dimethyl-3-nitrophenol, 360 g. potassium carbonate, 326 ml. benzyl chloride and 2 liters dimethyl formamide is stirred overnight at 50° C. The reaction mixture is then filtered with suction and the filtrate is evaporated to dryness in a vacuum. The residue is poured on to 4 liters of ice-water and, after suction filtration and drying in the air, there are obtained 668 g. of yellowish crystals; m.p. 66°-68° C.

WORKUP

后处理

  1. additionA mixture of 433 g
  2. filtrationThe reaction mixture is then filtered with suction
  3. customthe filtrate is evaporated to dryness in a vacuum
  4. additionThe residue is poured on to 4 liters of ice-water
  5. filtrationafter suction filtration
  6. customdrying in the air, there
  7. customare obtained 668 g