HRID426838
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of 433 g. 2,5-dimethyl-3-nitrophenol, 360 g. potassium carbonate, 326 ml. benzyl chloride and 2 liters dimethyl formamide is stirred overnight at 50° C. The reaction mixture is then filtered with suction and the filtrate is evaporated to dryness in a vacuum. The residue is poured on to 4 liters of ice-water and, after suction filtration and drying in the air, there are obtained 668 g. of yellowish crystals; m.p. 66°-68° C.
WORKUP
后处理
- additionA mixture of 433 g
- filtrationThe reaction mixture is then filtered with suction
- customthe filtrate is evaporated to dryness in a vacuum
- additionThe residue is poured on to 4 liters of ice-water
- filtrationafter suction filtration
- customdrying in the air, there
- customare obtained 668 g