4-Chloro-1-fluoro-2-nitrobenzene → HCID 20387677, compound

HRID 427030Notes

Reaction equation

HRID 427030 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5](F)=[C:6]([N+:8]([O-:10])=[O:9])[CH:7]=1.[NH2:12][C:13]1[CH:17]=[CH:16][S:15][C:14]=1[C:18]([O:20][CH3:21])=[O:19]>CCOC(C)=O.CCCCCC>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([NH:12][C:13]2[CH:17]=[CH:16][S:15][C:14]=2[C:18]([O:20][CH3:21])=[O:19])=[C:6]([N+:8]([O-:10])=[O:9])[CH:7]=1

Participants

4

Reactant 2

HCID 676604-Chloro-1-fluoro-2-nitrobenzeneHCID 89652Methyl 3-amino-2-thiophenecarboxylate

Product 1

HCID 20387677HCID 20387677, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

5-Chloro-2-fluoro-nitrobenzene and methyl 3-amino-thiophene-2-carboxylate, m.p. 207°-208° C. (EtOAc/Hexane).

Sources & evidence

ORD record
ord-c39e2defe753464cb662a2c5043a7a81
Source dataset
uspto-grants-1979_10
Patent number
US04172831

Reaction notes

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