Dihexylamine → HCID 18356286, compound

HRID 429506Notes

Reaction equation

[C:1]1(O)[CH:8]=[C:6]([CH3:7])[CH:5]=[C:3]([OH:4])[CH:2]=1.[CH2:10]([NH:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]>>[CH2:17]([N:16]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:1]1[CH:2]=[C:3]([OH:4])[CH:5]=[C:6]([CH3:7])[CH:8]=1)[CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

Participants

Reactant 2

HCID 8920Dihexylamine

HCID 10436Orcinol

Product 1

HCID 18356286HCID 18356286, compound

Procedure

Orcinol (5-resorcinol) was aminized by di-n-hexylamine, so as to obtain 1-di-n-hexylamino-3-methyl-5-hydroxybenzene. The hydroxy group thereof was etherized with methyl iodide, and then nitrosoized so as to obtain 1-di-n-hexylamino-3-methyl-4-nitroso-5-methoxybenzene.

Sources & evidence

ORD record: ord-3b366d82d196420a9bd95ad4ab7820fd
Source dataset: uspto-grants-2001_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06316605B1

Reaction notes

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