Trifluoromethanesulfonic acid → HCID 11000413, compound

HRID 430634Notes

Reaction equation

HRID 430634 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([F:8])[N:3]=1.[F:9][C:10]([F:16])([F:15])[S:11]([OH:14])(=[O:13])=[O:12]>>[F:9][C:10]([F:16])([F:15])[S:11]([O-:14])(=[O:13])=[O:12].[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([F:8])[N+:3]=1[CH3:10]

Participants

3

Reactant 2

HCID 62406Trifluoromethanesulfonic acidHCID 739342,6-Difluoropyridine

Product 1

HCID 11000413HCID 11000413, compound

Procedure

10 mmol of 2,6-difluoropyridine and 10 mmol of trifluoromethanesulphonic acid are mixed in a 50 ml round-bottomed flask and the mixture is stirred for 1 hour at ambient temperature under a nitrogen atmosphere. The white solid obtained is used directly in the following reaction without further purification.

Workup

  1. customThe white solid obtained
  2. customis used directly in the following reaction without further purification

Sources & evidence

ORD record
ord-c1a8567609c84e0f9f6bf18d3ba09fc2
Source dataset
uspto-grants-2001_11
Patent number
US06323220B1

Reaction notes

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