HRID430916

反应详情

EQUATION

反应方程式

HRID 430916 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

PAC is produced by adding 9-anthacenemethanol and pyridine to a solution of p-nitrophenyl chloroformate. Product is isolated to provide a crude anthrylmethyl p-nitrophenyl carbonate, which is then added to a solution of piperazine. The reacted mixture is poured into water and extracted with a solvent, preferably an organic solvent such as toluene. The product is washed and dried to provide 9-anthracenylmethyl-1-piperazinecarboxylate (PAC).

WORKUP

后处理

  1. customProduct is isolated
  2. customto provide a crude anthrylmethyl p-nitrophenyl carbonate, which
  3. extractionextracted with a solvent
  4. washThe product is washed
  5. customdried