反应详情

Into a 25 ml round bottom flask equipped with magnetic stirrer, thermometer, water bath, and reflux condenser is added a solution containing 0.27 g of sodium methoxide (0.005 moles) in 3 ml. absolute methanol. While maintaining the solution at 25° - 30° C., 0.57 g (0.005 moles) of 2-methyl-3-furan thiol in 2 ml of absolute methanol is added thereto. At 25° C., 0.483 g (0.005 moles) of chloromethyl methyl sulfide having the formula:

1. customInto a 25 ml round bottom flask equipped with magnetic stirrer
2. temperaturethermometer, water bath, and reflux condenser
3. additionis added a solution
4. temperatureWhile maintaining the solution at 25° - 30° C.
5. customAt 25° C.