HRID445217
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Add a solution of hydrogen chloride in ether (1.0 M, 5.5 mL, 5.50 mmol) to a solution of 6-methoxy-1-(4-(2-(piperidin-1-yl)ethoxy)phenoxy)naphthalen-2-yl trifluoromethanesulfonate (2.62 g, 4.99 mmol) and dichloromethane (20 mL). Stir the mixture for 10 minutes and then concentrate to obtain the title compound (2.8 g, 4.99 mmol).
WORKUP
后处理
- concentrationconcentrate