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HRID44644

反应详情

EQUATION

反应方程式

HRID 44644 的结构方程式

REACTANTS

反应物

2
结构：CN1CCNCC1
HCID53167

1-Methylpiperazine

C5H12N2

结构：COC(=O)c1cc([N+](=O)[O-])ccc1F
HCID11217860

METHYL 2-FLUORO-5-NITROBENZOATE

C8H6FNO4

PRODUCTS

生成物

1
结构：COC(=O)c1cc([N+](=O)[O-])ccc1N1CCN(C)CC1
HCID36405266

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of methyl 2-fluoro-5-nitro-benzoate (3.487 g, 17.511 mmol) and N-methylpiperazine (3.855 mL, 3.508 g, 35.022 mmol) in 30 mL of anhydrous methanol was heated to reflux for 5 hours.

WORKUP

后处理

  1. temperatureto reflux for 5 hours