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HRID460226

反应详情

EQUATION

反应方程式

HRID 460226 的结构方程式

REACTANTS

反应物

3
结构：C1CCOC1
HCID8028

Tetrahydrofuran

C4H8O

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CCOC(=O)c1csc(-c2ccc3c(cnn3C(C)=O)c2)n1
HCID69411765

未命名化合物

PRODUCTS

生成物

2
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：CC(=O)n1ncc2cc(-c3nc(C(=O)O)cs3)ccc21
HCID18772050

未命名化合物

PROCEDURE

实验过程

In a manner similar to Preparation CW from 2-(1-acetyl-1H-indazol-5-yl)-thiazole-4-carboxylic acid ethyl ester to give 2-(1-acetyl-1H-indazol-5-yl)-thiazole-4-carboxylic acid as a yellow solid following re-protection with Ac2O, Et3N, and THF. MS m/z: 286.1 (M−H). Calc'd for C13H9N3O3S 287.29.