Hydrochloric Acid → HCID 20476829, compound

HRID 461168Notes

Reaction equation

HRID 461168 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:12])[CH:9]=[N+]=[N-])=[CH:4][C:3]=1[S:13](=[O:17])(=[O:16])[NH:14][CH3:15].[ClH:18]>COCCOCCOC>[Cl:18][CH2:9][C:8]([C:5]1[CH:6]=[CH:7][C:2]([Cl:1])=[C:3]([S:13](=[O:17])(=[O:16])[NH:14][CH3:15])[CH:4]=1)=[O:12]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 54205136HCID 54205136, compound

Product 1

HCID 20476829HCID 20476829, compound

Reagents, catalysts & solvents 1

HCID 8150DiglymeSolvent

Procedure

12 g of 4'-chloro-3'-methylsulfamoyl-diazoacetophenone were reacted as prescribed in Example 66b) with concentrated HCl in diethyleneglycol dimethyl ether und worked up. Colorless crystals, melting point: 153° C.

Sources & evidence

ORD record
ord-d63069714ab44275952e4855a9943724
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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