Hydrochloric Acid → HCID 22760643, compound

HRID 461201Notes

Reaction equation

HRID 461201 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:12])[CH:9]=[N+]=[N-])=[CH:4][C:3]=1[S:13](=[O:20])(=[O:19])[N:14]([CH2:17][CH3:18])[CH2:15][CH3:16].[ClH:21]>COCCOCCOC>[CH2:15]([N:14]([CH2:17][CH3:18])[S:13]([C:3]1[CH:4]=[C:5]([C:8](=[O:12])[CH2:9][Cl:21])[CH:6]=[CH:7][C:2]=1[Cl:1])(=[O:20])=[O:19])[CH3:16]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 53853239HCID 53853239, compound

Product 1

HCID 22760643HCID 22760643, compound

Reagents, catalysts & solvents 1

HCID 8150DiglymeSolvent

Procedure

12 g of 4'-chloro-3'-diethylsulfamoyl-diazoacetophenone were reacted as prescribed in Example 66b) with concentrated HCl in diethyleneglycol dimethyl ether and worked up. Colorless crystals, melting point: 63° - 65° C.

Sources & evidence

ORD record
ord-722fc3f96a754c4cb3858824f922cfde
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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