Hydrochloric Acid → HCID 22760497, compound

HRID 461204Notes

Reaction equation

HRID 461204 reaction equation
[CH2:1]([N:5]([CH2:19][CH2:20][CH2:21][CH3:22])[S:6]([C:9]1[CH:10]=[C:11]([CH:15]=[CH:16][C:17]=1[Cl:18])C(Cl)=O)(=[O:8])=[O:7])[CH2:2][CH2:3][CH3:4].[N+](=C)=[N-].[ClH:26].C([O:29][CH2:30][CH3:31])C>COCCOCCOC>[CH2:1]([N:5]([CH2:19][CH2:20][CH2:21][CH3:22])[S:6]([C:9]1[CH:10]=[C:11]([C:30](=[O:29])[CH2:31][Cl:26])[CH:15]=[CH:16][C:17]=1[Cl:18])(=[O:7])=[O:8])[CH2:2][CH2:3][CH3:4]

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 9550DiazomethaneHCID 22760620HCID 22760620, compound

Product 1

HCID 22760497HCID 22760497, compound

Reagents, catalysts & solvents 1

HCID 8150DiglymeSolvent

Procedure

18 g of the 3-di-n-butylsulfamoyl-4-chlorobenzoylchloride so obtained as an oil were reacted as prescribed in Example 70c) in diethyl ether with diazomethane and then with concentrated HCl in diethyleneglycol dimethyl ether and worked up, 3'-di-n-butylsulfamoyl-2,4'-dichlororacetophenone being obtained in the form of colorless crystals having a melting point of 71° C.

Workup

  1. customwere reacted
  2. custom3'-di-n-butylsulfamoyl-2,4'-dichlororacetophenone being obtained in the form of colorless crystals

Sources & evidence

ORD record
ord-e9a37fe926314f1fa76f312c0551667f
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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