1-Bromooctane → HCID 131710970, compound

HRID 461453Notes

Reaction equation

HRID 461453 reaction equation
[CH2:1]([N:13]1[CH:17]=[CH:16][N:15]=[C:14]1[CH3:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:19]([Br:27])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>C(O)CC>[Br-:27].[CH2:1]([N:13]1[CH:17]=[CH:16][N:15]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[CH:14]1[CH3:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 81401-BromooctaneHCID 150999061-Dodecyl-2-methyl-1H-imidazole

Product 1

HCID 131710970HCID 131710970, compound

Reagents, catalysts & solvents 1

HCID 10311-PropanolSolvent

Conditions

Temperature
100 °C

Procedure

1 mole of 1-n-dodecyl-2-methylimidazole is dissolved in 500 ml of n-propanol and reacted with 1.1 moles of n-octyl bromide. The reaction mixture is heated at 100° C for 5 hours. Upon removing the solvent, the remaining residue is washed with ether, suctioned off, and dried.

Workup

  1. customUpon removing the solvent
  2. washthe remaining residue is washed with ether
  3. customdried

Sources & evidence

ORD record
ord-44e5ca79671743988aaee8a5085562a7
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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