1-Bromooctane → HCID 131710971, compound

HRID 461454Notes

Reaction equation

HRID 461454 reaction equation
[CH3:1][C:2]1[N:3]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH:4]=[CH:5][N:6]=1.[CH2:23]([Br:31])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]>C(O)(C)C>[Br-:31].[CH2:7]([N:3]1[CH:4]=[CH:5][N:6]([CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])[CH:2]1[CH3:1])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

Participants

4

Reactant 2

HCID 81401-BromooctaneHCID 21331298HCID 21331298, compound

Product 1

HCID 131710971HCID 131710971, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

0.5 mole of 2-methyl-1-n-hexadecylimidazole is dissolved in 250 ml of i-propanol and reacted with 0.6 mole of n-octyl bromide. This is followed by a 10-hour boiling with reflux. Then the i-propanol is distilled off, together with the unreacted n-octyl bromide, and the remaining residue is washed with ether.

Workup

  1. waitThis is followed by a 10-hour
  2. temperaturewith reflux
  3. distillationThen the i-propanol is distilled off, together with the unreacted n-octyl bromide
  4. washthe remaining residue is washed with ether

Sources & evidence

ORD record
ord-4fdca883e96a4372989a2c4ee03a04c7
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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