1-Bromooctane → HCID 21393911, compound

HRID 461455Notes

Reaction equation

HRID 461455 reaction equation
[CH2:1]([N:9]1[CH:13]=[CH:12][N:11]=[C:10]1[CH3:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH2:15]([Br:23])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>C(O)CC>[Br-:23].[CH2:1]([N:9]1[CH:13]=[CH:12][N:11]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH:10]1[CH3:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 81401-BromooctaneHCID 2310563660964-49-0

Product 1

HCID 21393911HCID 21393911, compound

Reagents, catalysts & solvents 1

HCID 10311-PropanolSolvent

Conditions

Temperature
105 °C

Procedure

1 mole of 1-n-octyl-2-methylimidazole is dissolved with 1.1 moles of n-octyl bromide in 500 ml of n-propanol and heated at 105° C for 5 hours. Then, the n-propanol together with the unreacted n-octyl bromide is distilled off and the remaining residue is washed with ether.

Workup

  1. distillationThen, the n-propanol together with the unreacted n-octyl bromide is distilled off
  2. washthe remaining residue is washed with ether

Sources & evidence

ORD record
ord-f40ff56797c14b2db899d4b43d95ac74
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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