1-Bromooctane → HCID 21393920, compound

HRID 461456Notes

Reaction equation

HRID 461456 reaction equation
[CH2:1]([N:9]1[CH:13]=[CH:12][N:11]=[C:10]1[CH2:14][CH3:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH2:16]([Br:24])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]>C(O)(C)C>[Br-:24].[CH2:1]([N:9]1[CH:13]=[CH:12][N:11]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])[CH:10]1[CH2:14][CH3:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 81401-BromooctaneHCID 21858034HCID 21858034, compound

Product 1

HCID 21393920HCID 21393920, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

0.6 mole of 1-n-octyl-2-ethylimidazole is dissolved in 250 ml of i-propanol and 0.66 mole of n-octyl bromide are boiled with reflux for 5 hours. The alcohol then is separated and the remaining residue is washed with ether.

Workup

  1. temperaturewith reflux for 5 hours
  2. customThe alcohol then is separated
  3. washthe remaining residue is washed with ether

Sources & evidence

ORD record
ord-5dc3adb55a254e3c903bc3479e798cec
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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