1-Bromooctane → HCID 86735280, compound

HRID 461459Notes

Reaction equation

HRID 461459 reaction equation
[CH2:1]([N:17]1[CH:21]=[CH:20][N:19]=[C:18]1[CH2:22][CH3:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:24]([Br:32])[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]>C(O)(C)C>[Br-:32].[CH2:1]([N:17]1[CH:21]=[CH:20][N:19]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31])[CH:18]1[CH2:22][CH3:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 81401-BromooctaneHCID 21331297HCID 21331297, compound

Product 1

HCID 86735280HCID 86735280, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

0.5 mole of 1-n-hexadecyl-2-ethylimidazole and 0.6 mole of n-octyl bromide are dissolved in 250 ml of i-propanol and boiled with reflux for 5 hours. The solvent then is separated and the residue washed with ether.

Workup

  1. temperaturewith reflux for 5 hours
  2. customThe solvent then is separated
  3. washthe residue washed with ether

Sources & evidence

ORD record
ord-134e82803dd44e03a1f6bf8373eb9574
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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