Salicylaldehyde → HCID 68122023, compound

HRID 461602Notes

Reaction equation

HRID 461602 reaction equation
[NH2:1][N:2]1[CH:6]=[N:5][N:4]=[CH:3]1.[CH:7](=O)[C:8]1[C:9](=[CH:11][CH:12]=[CH:13][CH:14]=1)[OH:10]>C1(C)C(C)=CC=CC=1>[CH:7](=[C:6]1[N:2]([NH2:1])[CH:3]=[N:4][NH:5]1)[C:8]1[C:9](=[CH:11][CH:12]=[CH:13][CH:14]=1)[OH:10]

Participants

4

Reactant 2

HCID 6998SalicylaldehydeHCID 114324-Amino-1,2,4-triazole

Product 1

HCID 68122023HCID 68122023, compoundYield 94.7%

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

4-amino-1,2,4-triazole (4.2 g.), salicylaldehyde (6.1g.) and xylene 140 ml. were heated at reflux for 3 hr. The reaction mixture was cooled and filtered to afford 9 grams of product, m.p. 210°-12°.

Workup

  1. temperaturewere heated
  2. temperatureat reflux for 3 hr
  3. temperatureThe reaction mixture was cooled
  4. filtrationfiltered

Sources & evidence

ORD record
ord-97895e036c774955b8816658d689d991
Source dataset
uspto-grants-1977_12
Patent number
US04064059

Reaction notes

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