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HRID462234

反应详情

EQUATION

反应方程式

HRID 462234 的结构方程式

REACTANTS

反应物

3
结构：C1CNCCN1
HCID4837

Piperazine

C4H10N2

结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

结构：Cn1c([N+](=O)[O-])cnc1C1=CNN(N2CCCCC2)S1
HCID21390837

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c([N+](=O)[O-])cnc1C1=CNN(N2CCNCC2)S1
HCID21390830

未命名化合物

PROCEDURE

实验过程

The preparation of the subject compound is carried out essentially as described for the 2-piperidino derivative (Example 28), two equivalents of piperazine replacing the piperidine. The crude project is recrystallized from 2-methoxyethanol to yield the pure compound melting at 240°-241° C. ;cl EXAMPLE 24

WORKUP

后处理

  1. customThe preparation of the subject compound
  2. customThe crude project is recrystallized from 2-methoxyethanol