Hydrochloric Acid → HCID 20282963, compound

HRID 463332Notes

Reaction equation

HRID 463332 reaction equation
[CH2:1]([C:4]1[C:10]([OH:11])=[CH:9][CH:8]=[CH:7][C:5]=1[OH:6])[CH2:2][CH3:3].Cl.C[CH2:14][O:15]CC>[C-]#N.[Zn+2].[C-]#N>[OH:11][C:10]1[C:4]([CH2:1][CH2:2][CH3:3])=[C:5]([OH:6])[CH:7]=[CH:8][C:9]=1[CH:14]=[O:15]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 2620601,3-Benzenediol, propyl-

Product 1

HCID 20282963HCID 20282963, compound

Reagents, catalysts & solvents 1

HCID 11186Zinc cyanide (Zn(CN)2)Catalyst

Procedure

Zinc cyanide (24 g) was added to a stirred suspension of 2-propylresorcinol (32.4 g) in dry ether (150 ml) and the resulting mixture saturated with hydrogen chloride. After being left to stand at room temperature for 30 minutes the ether was decanted and the remaining solid heated on the steam bath with water for 30 minutes.

Workup

  1. waitAfter being left
  2. customthe ether was decanted
  3. temperaturethe remaining solid heated on the steam bath with water for 30 minutes

Sources & evidence

ORD record
ord-a476cc4dec6746e3930204f21f8db795
Source dataset
uspto-grants-1985_05
Patent number
US04518612

Reaction notes

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