反应详情

In a similar manner 0.16 moles of triethylamine, 0.05 moles of PSBr3 and 150 milliliters of dried tetrahydrofuran are combined in a 250 milliliter round bottom flask which is thereafter treated with a first solution containing 0.10 moles of 2,2-dimethylaziridine in 20 milliliters of THF and a second solution containing 0.16 moles of dimethylamine in 25 millimeters of dried THF, to produce a slurry which after filtration, concentration of the filtrate and vacuum distillation affords about 65% yield of P,P-bis(2,2-dimethyl-1-aziridinyl)-N,N-dimethylthiophosphinic amide.

1. additionwhich is thereafter treated with a first solution
2. customto produce a slurry which
3. filtrationafter filtration, concentration of the filtrate and vacuum distillation