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HRID465074

反应详情

EQUATION

反应方程式

HRID 465074 的结构方程式

REACTANTS

反应物

3
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：O=C1Nc2cccnc2N(C(=O)CCl)c2ccccc21
HCID120053

11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-one

C14H10ClN3O2

结构：C1CN[C@H](CN2CCCC2)C1
HCID853152

未命名化合物

PRODUCTS

生成物

1
结构：O=C1Nc2cccnc2N(C(=O)CN2CCC[C@H]2CN2CCCC2)c2ccccc21
HCID13578576

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

The title compound is prepared analogously to Example 31 from 11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and (S)-(+)-2-[(1-pyrrolidinyl)methyl]pyrrolidine to give colorless crystals, mp. 192°-193° C. (ethyl acetate). [α]D20 =-18.1° (ethanol).