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HRID46706

反应详情

EQUATION

反应方程式

HRID 46706 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)O)cc1
HCID6101

4-Methylbenzenesulfonic acid

C7H8O3S

结构：CC(C)C(O)(c1ccccc1)c1ccc2nc(N)n(S(=O)(=O)N(C)C)c2c1
HCID20490458

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)=C(c1ccccc1)c1ccc2nc(N)n(S(=O)(=O)N(C)C)c2c1
HCID20490457

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

When the procedure of Example 72 was repeated using 1.2 g. (3.2 mmoles) of 1-dimethylaminosulfonyl-2-amino-6-(α-isopropyl-α-hydroxybenzyl)benzimidazole, 750 mg. of p-toluenesulfonic acid, and 100 ml. of chloroform, there was obtained 1-dimethylaminosulfonyl-2-amino-6-(α-isopropylidenebenzyl)benzimidazole.