HRID471390

反应详情

EQUATION

反应方程式

HRID 471390 的结构方程式

PROCEDURE

实验过程

The title compound is synthesized according to general procedure GP1 starting from 4.8 g (30 mmol) 6-trifluoromethyl-pyridin-2-ylamine and 6.7 g (30 mmol) NIS. Yield after precipitation from the reaction mixture and isolation of additional product from the mother liquid by chromatography in silica gel: 5.73 g (67%).

WORKUP

后处理

  1. customYield
  2. customafter precipitation from the reaction mixture and isolation of additional product from the mother liquid by chromatography in silica gel