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HRID472360

反应详情

EQUATION

反应方程式

HRID 472360 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)N=C=S
HCID85320

Ethyl isothiocyanatoformate

C4H5NO2S

结构：Cl.NO
HCID443297

未命名化合物

结构：Nc1ncc(C(F)(F)F)cc1Br
HCID13064155

3-Bromo-5-(trifluoromethyl)pyridin-2-amine

C6H4BrF3N2

PRODUCTS

生成物

1
结构：Nc1nc2c(Br)cc(C(F)(F)F)cn2n1
HCID67481469

未命名化合物

PROCEDURE

实验过程

8-Bromo-6-trifluoromethyl-[1,2,4]triazolo[1,5-a]pyridin-2-ylamine was prepared from 3-bromo-5-trifluoromethyl-pyridin-2-ylamine, ethoxycarbonylisothiocyanate, and hydroxylamine hydrochloride in a manner analogous to Steps 2a-b. 1H NMR (400 MHz, (D3C)2SO, δ, ppm): 9.24 (s, 1H), 8.08 (s, 1H), 6.62 (bs, 2H). MS=282.9 (MH)+.