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HRID47300

反应详情

EQUATION

反应方程式

HRID 47300 的结构方程式

REACTANTS

反应物

3
结构：C1CCC2=NCCCN2CC1
HCID81184

1,8-Diazabicyclo[5.4.0]undec-7-ene

C9H16N2

结构：N#Cc1ccc2c(Cl)nnc(Cl)c2c1
HCID10656738

1,4-dichlorophthalazine-6-carbonitrile

C9H3Cl2N3

结构：COc1ccc(CN)cc1C#N
HCID22744645

5-(Aminomethyl)-2-methoxybenzonitrile

C9H10N2O

PRODUCTS

生成物

1
结构：COc1ccc(CNc2nnc(Cl)c3ccc(C#N)cc23)cc1C#N
HCID86588311

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN1CCCC1=O
溶剂HCID13387

N-Methyl-2-pyrrolidone

C5H9NO

PROCEDURE

实验过程

1,4-Dichlorophthalazine-6-carbonitrile and 3-cyano-4-methoxybenzylamine were stirred at room temperature in 1-methyl-2-pyrrolidinone in the presence of DBU, whereby 1-chloro-4-[(3-cyano-4-methoxybenzyl)amino]-6-phthalazine carbonitrile was obtained as a less polar product.