HRID474003

反应详情

EQUATION

反应方程式

HRID 474003 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of tert-butyl 3-cyano-3-methylazetidine-1-carboxylate (30.0 mg, 0.15 mmol) in dichloromethane (5 ml) was added trifluoroacetic acid (2 ml) and the solution stirred at room temperature for 1 hr. The reaction was concentrated and dried under vacuum to give a viscous oil which was used crude in subsequent chemistry.

WORKUP

后处理

  1. concentrationThe reaction was concentrated
  2. customdried under vacuum
  3. customto give a viscous oil which