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HRID476208

反应详情

EQUATION

反应方程式

HRID 476208 的结构方程式

REACTANTS

反应物

2
结构：CCOC(C)=S
HCID136711

Thioacetic acid, O-ethyl ester

C4H8OS

结构：COc1cc(/C=C/C(=O)O)ccc1O[Si](C)(C)C(C)(C)C
HCID11185931

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=S)CC(=O)/C=C/c1ccc(O[Si](C)(C)C(C)(C)C)c(OC)c1
HCID131731171

未命名化合物

收率 60%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The title compound was prepared in the same manner as in Step 1 of Example C-1, except that an equimolar amount of each of trans-3-methoxy-4-tert-butyldimethylsilyloxy-cinnamic acid prepared in Step 1 of Example C-10 and ethyl thioacetate was used in place of trans-cinnamic acid and ethyl acetate.