HRID481498
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of Compound 18 (280 mg) in AcOEt (6 ml) was added conc. HCl (1 ml). The mixture was stirred at room temperature for 45 minutes. The mixture was extracted with CH2Cl2. The combined extracts were dried (Na2SO4), and concentrated in vacuo to give Compound 19 as a yellow oil.
WORKUP
后处理
- extractionThe mixture was extracted with CH2Cl2
- dry with materialThe combined extracts were dried (Na2SO4)
- concentrationconcentrated in vacuo