Acetone → HCID 13532059, compound

HRID 485401Notes

Reaction equation

HRID 485401 reaction equation
[OH:1][CH:2]([C:7](=[O:20])[C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][CH2:16][CH:17]([CH3:19])[CH3:18])=[CH:10][CH:9]=1)S(O)(=O)=O.[Na].Cl.CC(C)=[O:25]>>[OH:1][CH:2]([OH:25])[C:7]([C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][CH2:16][CH:17]([CH3:19])[CH3:18])=[CH:10][CH:9]=1)=[O:20]

Participants

5

Reactant 4

HCID 180AcetoneHCID 313Hydrochloric AcidHCID 5360545SodiumHCID 20270503HCID 20270503, compound

Product 1

HCID 13532059HCID 13532059, compound

Procedure

A 6.0 g. portion of hydroxy [p-(isopentyloxy)benzoyl]methanesulfonic acid, sodium salt was dissolved in a mixture of 100 ml. of 0.5N hydrochloric acid and 15 ml. of acetone. The solid was collected, giving the desired product, m.p. 80°-85° C.

Workup

  1. customThe solid was collected

Sources & evidence

ORD record
ord-c5db11ebad8c4cb39b68cebdfba1317d
Source dataset
uspto-grants-1985_08
Patent number
US04536517

Reaction notes

Loading…