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HRID487541

反应详情

EQUATION

反应方程式

HRID 487541 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)CBr
HCID7748

Ethyl bromoacetate

C4H7BrO2

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：O=C1C(Cc2ccncc2)c2ccccc2N1N1CCOCC1
HCID23353976

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CC1(Cc2ccncc2)C(=O)N(N2CCOCC2)c2ccccc21
HCID86747675

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.ClC(Cl)Cl
溶剂HCID21585165

未命名化合物

PROCEDURE

实验过程

The product obtained from Example 20 could be reacted with sodium hydride and ethyl bromoacetate in a manner similar to Example 8 to render the product as a crystalline white solid, m.p. 168°-2/3° C. (hexane-chloroform). High Res. Mass Spec. Calcd. for C22H25N3O4 : 396.1923 (M+H). Found: 396.1922.