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HRID488493

反应详情

EQUATION

反应方程式

HRID 488493 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)Cc1ccc([N+](=O)[O-])cc1
HCID4661

4-Nitrophenylacetic acid

C8H7NO4

结构：COc1cc(C=O)cc(OC)c1OC
HCID6858

Benzaldehyde, 3,4,5-trimethoxy-

C10H12O4

结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

PRODUCTS

生成物

1
结构：COc1cc(C=Cc2ccc([N+](=O)[O-])cc2)cc(OC)c1OC
HCID54348404

未命名化合物

收率 41%

PROCEDURE

实验过程

The title compound was prepared from p-nitrophenylacetic acid (18.6 g, 0.10 mol), 3,4,5-trimethoxy-benzaldehyde (19.6 g, 0.10 mol) and piperidine (5 mL) using the procedure described in Example 1, Step A. This procedure yielded a solid, 13.0 g (0.041 mol, 41%) of the desired product. mp: 192-195° C.