HRID49038

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C(O)C1CN(C(=O)OCc2ccccc2)CCN1c1c([N+](=O)[O-])ccc(Cl)c1Cl

HCID21976687

未命名化合物

PRODUCTS

生成物

结构：O=C1Nc2ccc(Cl)c(Cl)c2N2CCN(C(=O)OCc3ccccc3)CC12

HCID21976679

未命名化合物

收率 50.7%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23925

Iron

PROCEDURE

实验过程

By the same procedure described for Example 7 B, from 0.75 g of 4-carbobenzyloxy-1-(5,6-dichloro-2-nitrophenyl)piperazine-2-carboxylic acid and 0.28 g of iron powder, there was obtained 0.34 g (49%) of the desired product as a brown solid.