Hydrochloric Acid → HCID 22320904, compound

HRID 498151Notes

Reaction equation

HRID 498151 reaction equation
Cl.[CH2:2]([O:12][CH2:13][CH2:14][CH2:15][C:16]1([C:21]2[CH:26]=[CH:25][C:24]([CH3:27])=[CH:23][CH:22]=2)OCC[O:17]1)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]>C1COCC1>[CH2:2]([O:12][CH2:13][CH2:14][CH2:15][C:16]([C:21]1[CH:26]=[CH:25][C:24]([CH3:27])=[CH:23][CH:22]=1)=[O:17])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22320887HCID 22320887, compound

Product 1

HCID 22320904HCID 22320904, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

This compound was synthesized as described under 5.c) with 4.4 ml of HCl (1N) and 4.33 g (11.9 mmol) of 2-[3-(decyloxy)propyl]-2-(4-methylphenyl)-1,3-dioxolane obtained under b) in 100 ml of THF to give 3.82 g (99%) of a slightly yellow oil that solidifies at 4°.

Workup

  1. customThis compound was synthesized
  2. customto give 3.82 g (99%) of a slightly yellow oil
  3. customthat solidifies at 4°

Sources & evidence

ORD record
ord-b5a3705ba49747eca90c965f4b910acd
Source dataset
uspto-grants-2005_09
Patent number
US06949680B2

Reaction notes

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