Hydrochloric Acid → HCID 22320893, compound

HRID 498152Notes

Reaction equation

HRID 498152 reaction equation
Cl.[CH3:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2([CH2:14][CH2:15][CH2:16][O:17][CH2:18][CH2:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)OCC[O:10]2)=[CH:5][CH:4]=1>C1COCC1>[CH3:2][C:3]1[CH:4]=[CH:5][C:6]([C:9](=[O:10])[CH2:14][CH2:15][CH2:16][O:17][CH2:18][CH2:19][C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=2)=[CH:7][CH:8]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22320906HCID 22320906, compound

Product 1

HCID 22320893HCID 22320893, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

This compound was synthesized as described under 5.c) with 2.3 ml of HCl (1N), 2.05 g (6.3 mmol) of 2-(4-methylphenyl)-2-[3-(phenylethoxy)propyl]-1,3-dioxolane obtained under a) in 50 ml of THF for 3 h to give 1.81 g (99%) of a slightly yellow oil that solidifies at 4° C.

Workup

  1. customThis compound was synthesized
  2. customto give 1.81 g (99%) of a slightly yellow oil
  3. customthat solidifies at 4° C.

Sources & evidence

ORD record
ord-5b5e98b6d9444aefa511058d5652ea40
Source dataset
uspto-grants-2005_09
Patent number
US06949680B2

Reaction notes

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