Hydrochloric Acid → HCID 22320903, compound

HRID 498154Notes

Reaction equation

HRID 498154 reaction equation
Cl.[C:2]([C:6]1[CH:11]=[CH:10][C:9]([C:12]2([CH2:17][CH2:18][CH2:19][O:20][CH2:21][CH2:22][C:23]3[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=3)OCC[O:13]2)=[CH:8][CH:7]=1)([CH3:5])([CH3:4])[CH3:3]>C1COCC1>[C:2]([C:6]1[CH:11]=[CH:10][C:9]([C:12](=[O:13])[CH2:17][CH2:18][CH2:19][O:20][CH2:21][CH2:22][C:23]2[CH:24]=[CH:25][CH:26]=[CH:27][CH:28]=2)=[CH:8][CH:7]=1)([CH3:5])([CH3:3])[CH3:4]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22320895HCID 22320895, compound

Product 1

HCID 22320903HCID 22320903, compoundYield 101%

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

This compound was synthesized as described under 5.c) with 2 ml of HCl (1N) and 2.00 g (5.4 mmol) of 2-(4-tert-butylphenyl)-2-[3-(2-phenylethoxy)propyl]-1,3-dioxolane obtained under b) in 50 ml of THF to give 1.77 g (99%) of a yellow oil.

Workup

  1. customThis compound was synthesized

Sources & evidence

ORD record
ord-622fa27119a5469aba293e36bd35d47e
Source dataset
uspto-grants-2005_09
Patent number
US06949680B2

Reaction notes

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