HRID499662

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID80972

Ethane, 1-bromo-2-methoxy-

C3H7BrO

HCID42625856

未命名化合物

PRODUCTS

生成物

结构：COCC[N+]12CCC(C(O)(c3ccccc3)c3ccccc3)(CC1)C2.[Br-]

HCID16041400

未命名化合物

收率 24.1%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Following the general procedure outlined in Example 1, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol (30.8 mg, 0.110 mmol) and 1-bromo-2-(methyloxy)ethane (0.03 mL, 0.3 mmol) in 2 CH3CN/3 CHCl3 (2.5 nm) were reacted to give the desired product (11.1 mg, 24%). EI-MS m/z 338 (M+) Rt (1.64 min).

WORKUP

后处理

customwere reacted