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HRID50239

反应详情

EQUATION

反应方程式

HRID 50239 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：O=C([O-])[O-].[NH4+].[NH4+]
HCID517111

Ammonium carbonate

CH8N2O3

结构：CN1CCC(N(C)S(=O)(=O)c2ccc3c(c2)nc(COc2ccc(C#N)cc2)n3C)CC1
HCID18412364

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCC(N(C)S(=O)(=O)c2ccc3c(c2)nc(COc2ccc(C(=N)N)cc2)n3C)CC1.Cl
HCID18412592

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 25d from 400 mg of 1-methyl-2-[(4-cyanophenyl)oxymethyl]benzimidazol-5-yl-sulfonic acid-N-methyl-N-(1-methylpiperidin-4-yl)amide with ethanolic hydrochloric acid and ammonium carbonate. Yield: 370 mg (83% of theory), C23H30N6O3S (470.6); EKA mass spectrum: (M+H)+=471; (M+2H)++=236.