HRID502637

反应详情

EQUATION

反应方程式

HRID 502637 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Into a 50 mL round bottom flask was placed 4-chloro-5-phenylfuro[2,3-d]pyrimidine, isopropanol (25 mL), and isopropylamine (1.5 g, 25 mmol). The flask was equipped with a magnetic stir bar, a reflux condenser, and argon balloon and the reaction was brought to reflux with stirring for 20 hours.

WORKUP

后处理

  1. customInto a 50 mL round bottom flask was placed
  2. customThe flask was equipped with a magnetic stir bar, a reflux condenser
  3. temperatureto reflux