4-Nitrophenol → HCID 28300928, compound

HRID 502747Notes

Reaction equation

[N+:1]([C:4]1[CH:5]=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)([O-])=O.[N+:11]([C:14]1[CH:19]=[CH:18][C:17](O)=[CH:16]C=1)([O-])=O.N1CC[CH2:24][CH2:23][CH2:22]1.Cl.CNC>>[N:11]1([CH2:22][CH2:23][CH2:24][O:10][C:6]2[CH:5]=[C:4]([CH:9]=[CH:8][CH:7]=2)[NH2:1])[CH2:14][CH2:19][CH2:18][CH2:17][CH2:16]1

Participants

Reactant 4

HCID 9804-Nitrophenol

HCID 8082Piperidine

HCID 10473Dimethylamine, hydrochloride

HCID 111373-Nitrophenol

Product 1

HCID 28300928HCID 28300928, compound

Procedure

The title compound was prepared by a method similar to that described in Example 154 above, wherein 3-nitrophenol was substituted for 4-nitrophenol in Step 1 and piperidine for dimethylamine hydrochloride in Step 2. MS (m/z)=235.2 (M+H+); Calc'd for C14H23N2O=234.34.

Sources & evidence

ORD record: ord-ede11181226a447b98a512fa34401fc9
Source dataset: uspto-grants-2010_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07776869B2

Reaction notes

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