1,4-Dibromobutane → HCID 68466912, compound

HRID 502950Notes

Reaction equation

HRID 502950 reaction equation
[C:1]1([CH2:7][C:8]#[N:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.Br[CH2:11][CH2:12][CH2:13][CH2:14]Br.[H-].[Na+]>CN(C=O)C>[C:1]1([C:7]2([C:8]#[N:9])[CH2:14][CH2:13][CH2:12][CH2:11]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1

Participants

5

Reactant 3

HCID 80561,4-DibromobutaneHCID 24758Sodium hydrideHCID 814611-Cyclohexene-1-acetonitrile

Product 1

HCID 68466912HCID 68466912, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Cyclohex-1-en-1-ylacetonitrile and 1,4-dibromobutane were reacted in DMF at room temperature in the presence of sodium hydride to obtain 1-cyclohex-1-en-1-ylcyclopentanecarbonitrile.

Sources & evidence

ORD record
ord-8bdd77f4eab14e69afe94aadf35d3298
Source dataset
uspto-grants-2010_08
Patent number
US07776897B2

Reaction notes

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