反应详情

A solution of methylamine in ethanol (10 mL, 80 mmol, 8M solution in ethanol) was added to a solution of Methyl 3-Bromo-2-(bromomethyl)benzoate in THF (30 mL). After stirring for 2 h the reaction mixture was concentrated to dryness and water (30 mL) was added with rapid stirring. The solids produced were isolated by filtration and dried to give the desired product

1. concentrationwas concentrated to dryness and water (30 mL)
2. additionwas added with rapid stirring
3. customThe solids produced
4. customwere isolated by filtration
5. customdried